Indonesian Journal of Fundamental and Applied Chemistry
Vol 1, No 1 (2016): February 2016

The influence of time reaction to characteristic of methyl ester sulfonate from seed oil ketapang

Hariani, Poedji Loekitowati (Unknown)
Riyanti, Fahma (Unknown)
Fadilah, Ahyati (Unknown)



Article Info

Publish Date
14 Sep 2016

Abstract

The aim of the present work was to The Preparation of Methyl Ester Sulfonate From Ketapang Seed Oil As Surfactant. The research is to determine the optimum condition synthesis of methyl ester sulfonate surfactant with reaction time variations (3.5; 4.0; 4.5; 5.0; 5.5 hours). The methyl ester from ketapang seed oil were analysis by GC-MS and identified methyl ester sulfonate by using FTIR spectroscopy. The methyl ester from ketapang seed oil showed containing of methyl palmitoleic, methyl linoleic, methyl palmitate, methyl stearate, methyl oleic, methyl palmitolenat and methyl eicosenoate. The optimum condition of methyl ester sulfonate at reaction time 4.5 hours with the mass of methyl ester sulfonate 34,85 g. For the FTIR spectra of sulfonate group is indicated  by shifting of wave number at 1118.71cm-1 until 1029.1 cm-1. The characteristics of methyl ester sulfonate at the optimum reaction time have emulsion stability 71.684%, density 0.8714 g/mL, surface tension 36.232 dyne/cm, and maximum absorbance 1.428 at the maximum wavelength 660 nm. Keywords: Surfactant, methyl ester sulfonate, time reaction, ketapang seed oil

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Journal Info

Abbrev

IJFAC

Publisher

Subject

Biochemistry, Genetics & Molecular Biology Chemistry Environmental Science

Description

Indonesian Journal of Fundamental and Applied Chemistry (IJFAC) is an international research journal and invites contributions of original research articles as well as review articles in several areas of chemistry. The journal aims to publish refereed, high-quality research papers with significant ...