Journal of Chemistry
Vol. 7, No. 2 Juli 2013

STUDI REAKSI SIKLOPENTILSILAN DENGAN 4-IODIDA THIOANISOL MENGGUNAKAN KATALIS PALADIUM

Lesbani, Aldes (Unknown)
Mohadi, Risfidian (Unknown)
Elfita, Elfita (Unknown)



Article Info

Publish Date
17 Jul 2013

Abstract

A study on cyclopentylsilane reaction in tetrahydrofuran with 4-iodo thioanisol has been carried out using palladium as catalyst under argon atmosphere at room temperature. The results showed that the product was tris(4-thioanisyl)cyclopentylsilane (1) which was obtained from recrystallization using methanol with the yield 35%. The Compound (1) has a melting point of 91.5-92.0 oC. Analysis using GC-MS found m/z 466 with six equivalent protons and eight carbons peak obtained from 1H and 13C NMR.

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Journal Info

Abbrev

jchem

Publisher

Subject

Biochemistry, Genetics & Molecular Biology Chemical Engineering, Chemistry & Bioengineering Chemistry Environmental Science Materials Science & Nanotechnology

Description

Jurnal Kimia (Journal of Chemistry) publishes papers on all aspects of fundamental and applied chemistry. The journal is naturally broad in scope, welcomes submissions from across a range of disciplines, and reports both theoretical and experimental studies. As well as original research, Jurnal ...