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Journal : Jurnal Iptek Nuklir Ganendra

SIMULATIONS ON NICKEL TARGET PREPARATION AND SEPARATION OF Ni(II)-

Jurnal Iptek Nuklir Ganendra Vol 14, No 1 (2011)
Publisher : BATAN

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Abstract

SIMULATIONS ON NICKEL TARGET PREPARATION AND SEPARATION.OF Ni(II)-Cu(II) MATRIX FORPRODUCTION OF RADIOISOTOPE64Cu64Ni (p,n) 64  and retained on the column while the nickel was kept in the form of Ni2+  2+  2+ and CuCl while the nickel was totally in the form of Ni2+  while the nickel was found as both Ni2+ and NiCl   while the nickel was mostly in the form of Ni2+. The retained CuCl was then changed back into Cu2+     Keywords 64 Cu, Anion exchange chromatography.: Nickel target preparation, Radioisotope Cu-64, Separation of Ni(II)-Cu(II) matrix, Nuclear reaction of 64Ni(p,n) cation form andeluted out the column by using HCl 0.05 M. The 42– 4 2–.The best condition of separation was in HCl 8 M in which the radioactive copper was mostly in the form of CuCl 42– 42– . In the condition ofHCl 9 M, the radioactive copper was mostly in the form of CuCl 42– cation. It was found that the electroplating result from the acidic solution was more satisfied than that from the basic solution. By conditioning the matrix solution at HCl 6 M, the radioactivecopper was found in the forms of Cucation and eluted off from the column. The retained radioactive copper was then eluted out the column in the condition of dilute HCl changingback the copper anion complex into Cu42– Cu. The nickel target preparation was performed by means of electroplating method using acidic solution of nickel chloride - boric acid mixture and basic solution of nickel sulphate – nickel chloridemixture on a silver- surfaced-target holder. The simulated solution of Ni(II) – Cu(II) matrix was considered as thesolution of post-proton-irradiated nickel target containing both irradiated nickel and radioactive copper, but in thepresented work the proton irradiation of nickel target was omitted, while the radioactive copper was originallyobtained from neutron irradiation of CuO target. The separation of radioactive copper from the nickel target matrixwas based on anion exchange column chromatography in which the radiocopper was conditioned to form anioncomplex CuClg-spectrometric analysis showed a single strong peak at 511 keVwhich is in accord to g-annihilation peak coming from positron decay of Cu-64, and a very weak peak at 1346 keVwhich is in accord to g-ray of Cu-64.. The simulations on Nickel target preparation and separation of Ni(II)- Cu(II) matrix has been carried out as a preliminary study for production of medical radioisotope Cu-64 based onnuclear reaction of

Co-Authors A. Isnansetyo, A. A.E.T.H. Wahyuni Abdul Muthalib Abidin Abidin Agus Cahyono Agus Nursalim, Agus Agustiar, Devie Ahmad, Hariyatunnisa ALIM ISNANSETYO Ambariyanto , Andriansyah, Rico Andrianus Andrianus, Andrianus Anik Rahmawati, Anik Anshor, Arrini Shabrina Anung Pujiyanto Ardiyawan, Ardiyawan Arief Taslihan Arief, Ahmad Fikri Astri Charolina Azmi, Azmi Azmi, Ulya Zakaria Basri, Novysa Basuki, Umar Beniarso, Mundin Cahyana Amiruddin Darfioes Basir Daya Agung Sarwono Desrina Desrina Desty Ratna Permatasari, Desty Ratna Dian Indriani Dini Siswani Mulia Dini, Tria Ayu Drajad Sarwo Seto, Drajad Sarwo Duranta D. Kembaren, Duranta D. Dwiningtyas, Ratih Dyah Indriyani, Putri E. Sarmini Edi Irawan Eko Sugiarto, Eko Endang Sarmini Enny Lestari Erik, Mohamad Erni Martani Ervia Yudiati FAJAR SETIAWAN Fatimah Azzahrah Fatmawati, Harlinda Fauziyah, Fuzi Afiza Finny Fitry Yani Fitriani Fitriani H. Syakuri, H. Habib Adjie Hadi, Muhammad Tesar Hambali Hambali Hartono Hartono Henny Ekana Ch. Henny Ekana Chrisnawati Herlina Herlina Hotnida Junita Situmeang Imamudin, Kurniasih INDAH ISTIQOMAH Irfan D. Prijambada Islami, Hidayatul Iswidiarti, Sri JAKA WIDADA K. H. Nitimulyo, K. H. Kadarisman Kadarisman Kamiso H. N., Kamiso H. KAMISO HANDOYO NITIMULYO KH, Abdul Aziz Kundharu Saddhono Kurniasih Kurniasih LANGKAH SEMBIRING Lantip Diat Prasojo Lestari, Fajar Sumi Lili Sholichah, Lili Ma'sum, Aziz Malarsih Malarsih, Malarsih Manik, Astri Marita Mardi Mardi Mardiyana Mardiyana Maria Ulfahmi, Cut Gesti Mayang Pitaloka MIFTAKHUL JANNAH Mirwa, Tetty Muh. Ibnan Syarif, Muh. Ibnan Muhammad Murdjani Muhammad Zainuddin Muhammmad Murdjani, Muhammmad Mujiyono Mujiyono Murti, Fahriza Murwantoko Murwantoko Namastra Probosunu Nina Yuliana Ningsih, Maya Nirmalasari Idha Wijaya Noer Kasanah, Noer Nur Fadhilah Nur Rokhmat Nursyirwani Nursyirwani Pratiwinindya, Ratih Ayu Prayogo, Sugeng Putri Puspitasari R Sudradjat, R Rachmansyah Rachmansyah Raden Bagus Sugio Sumanta Ratna Puspita, Ratna REZA Adi ADI PRADANA Risca Damayanti, Risca Risnawati, Ririn Riyadi Riyadi Rukayah Rukayah S. Soenarjo Sabillah, Masayu Selly Sahli, Zamahsjari Salu, Vega Ricky SANTI NURBAITI Sebastian Margino Sesung, Rusdiyanto Setyaningrum, Ikha Sulis Setyobudi Setyobudi Shanie, Arsan Shatrie, Dikry N Shatrie, Dikry Novel Siti Amirah Budiastuti Sri Hartati Sri Iswidayati Sri Rejeki Sriyono Sriyono Subagiyo Subagiyo Suharno Suharno Suherman Suherman Sumarwati Sumarwati Sumaryanto Florentinus, Totok Sunarhadijoso Soenarjo Sunarto Sunarto Suparti Suparti Sutarman Sutarman Sutrisno sutrisno Suyono Suyono syakir syakir Syarif, Muh Ibnan Tanjung, Dailami Tjetjep Rohendi Rohidi, Tjetjep Rohendi Totok Sumaryanto Florentinus, Totok Sumaryanto Totok Sumaryanto, Totok Triani Widyaningrum Udi Utomo Umi Nur Sholikhah W. Asmara W.Y. Rahman Wadiyo Wadiyo, Wadiyo Wardani, Anestia Widya Widaningtyas H, Adoniati Meyria Wijaya, Dhimayu Ichtiara Wilis Ari Ari Setyati1,2, Wilis Ari Wilis Ari Setyati Windi Amelia, Windi Wira Rahman Wira Y. Rahman Wisnu Nurcahyo Wulandari, Tita Yudha Trinoegraha Adiputra Yulius Docang Casessar Yuniarti, Ivana