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Journal : Atom Indonesia Journal

Separation of Radiocopper 64/67Cu from the Matrix of Neutron-Irradiated Natural Zinc Applicable for 64Cu Production Soenarjo, S.; Sriyono, Sriyono; Rahman, W.Y.; Sarmini, E.; Hambali, Hambali; Triyanto, Triyanto
Atom Indonesia Vol 38, No 1 (2012): April 2012
Publisher : PPIKSN-BATAN

Show Abstract | Download Original | Original Source | Check in Google Scholar | Full PDF (237.644 KB) | DOI: 10.17146/aij.2012.136

Abstract

Radioisotope 64Cu is a promising radiometallic-isotope for molecular-targeted-radiopharmaceuticals. Having a half-life of 12.70 hours and emitting β+-radiation (Eβ+ = 0.6531 MeV) as well as β-ray (Eβ- = 0.5787 MeV), it is widely used in the form of biomedical-substrate-radiopharmaceutical for positron emission tomography (PET) diagnosis and simultaneously for targeted radiotherapy of cancer. The potential needs on the availability of 64Cu-labeled pharmaceuticals for domestic nuclear medicine hospitals lead to a necessity for the local production of carrier-free 64Cu using BATAN’s G.A. Siwabessy reactor because of the technical and economical constraints in the production using BATAN’s cyclotron. The presented work is accordingly to study whether the radioisotope 64Cu can be produced and separated from the matrix of post-neutron-irradiated-natural zinc. This study is expected can be further improved and implemented in production technology of carrier-free 64Cu based on 64Zn (n,p) 64Cu nuclear reaction exploiting the fast neutron fraction among the major thermal fraction due to unavailability of fast-neutron-irradiation facility in the BATAN’s G.A. Siwabessy reactor. The solution of post-neutron-irradiated-natural zinc in 1M acetic acid was loaded into Chelex-100 cation exchanger resin column to pass out the Zn/Zn* fraction whereas the Cu* fraction which remained in the column was then eluted out from the column by using 1.5 M HCl and loaded into the second column containing Dowex-1X8 anion exchanger resin. The second column was then eluted with 0.5 M HCl. The collected eluate was expected to be zinc-free Cu* fraction. It was observed from the half-life and the γ-spectrometric analysis that radioactive copper-64Cu containing 67Cu was produced by neutron activation on the natural Zn-foil target and can be separated from the target matrix by the presented two-steps-column-chromatographic separation technique. The radioactivity measurement showed that wrapping the Zn target with cadmium foil increased the activity of radioactive copper and, thus, the Cu*/Zn*-ratio.Received: 28 June 2011; Revised: 21 February 2012; Accepted: 24 February 2012
Co-Authors A. Isnansetyo, A. A.E.T.H. Wahyuni Abdul Muthalib Abidin Abidin Afi Tarmiawati Agus Cahyono Agus Nursalim, Agus Agustiar, Devie Ahmad, Hariyatunnisa ALIM ISNANSETYO Ambariyanto , Andriansyah, Rico Andrianus Andrianus, Andrianus Andriyani, Fanata Anik Rahmawati, Anik Anshor, Arrini Shabrina Anung Pujiyanto Ardiyawan, Ardiyawan Arief Taslihan Arief, Ahmad Fikri Astri Charolina Azmi, Azmi Azmi, Ulya Zakaria Basri, Novysa Basuki, Umar Beniarso, Mundin Cahyana Amiruddin Ciswiyati, Dwi Endah Darfioes Basir Daya Agung Sarwono Desrina Desrina Desty Ratna Permatasari, Desty Ratna Dian Indriani Dimas A. Pamungkas Dini Siswani Mulia Dini, Tria Ayu Diniarti, Eka Drajad Sarwo Seto, Drajad Sarwo Duranta D. Kembaren, Duranta D. Dwiningtyas, Ratih Dyah Indriyani, Putri E. Sarmini Edi Irawan Eko Sugiarto, Eko Endang Sarmini Enny Lestari Erik, Mohamad Erni Martani Ervia Yudiati FAJAR SETIAWAN Fatimah Azzahrah Fatmawati, Harlinda Fauziyah, Fuzi Afiza Finny Fitry Yani Fitriani Fitriani Gunadi Gunadi H. Syakuri, H. Habib Adjie Hadi, Muhammad Tesar Hambali Hambali Hariswari, Kadek Paramitha Hartono Hartono Henny Ekana Ch. Henny Ekana Chrisnawati Herimanto Herimanto Herlina Herlina Hotnida Junita Situmeang Imamudin, Kurniasih INDAH ISTIQOMAH Irfan D. Prijambada Islami, Hidayatul Istanto, Riza Iswidiarti, Sri JAKA WIDADA Jazuli, Jazuli Juraida, Irma K. H. Nitimulyo, K. H. Kadarisman Kadarisman Kamiso H. N., Kamiso H. KAMISO HANDOYO NITIMULYO Kartikasari, Aprilia KH, Abdul Aziz Kundharu Saddhono Kurniasih Kurniasih LANGKAH SEMBIRING Lantip Diat Prasojo Lelana, Dewi Barata Siswa Lestari, Fajar Sumi Lestari, Yeni Sri Lili Sholichah, Lili Ma'sum, Aziz Malarsih Malarsih, Malarsih Manik, Astri Marita Mardi Mardi Mardiyana Mardiyana Maria Ulfahmi, Cut Gesti Mariana, Zulfa Mayang Pitaloka MIFTAKHUL JANNAH Mirwa, Tetty Muh. Ibnan Syarif, Muh. Ibnan Muhamad Aris Widodo Muhammad Murdjani Muhammad Zaini Muhammad Zainuddin Muhammmad Murdjani, Muhammmad Mujiyono Mujiyono Murti, Fahriza Murtiyoso, Onang Murwantoko Murwantoko Musa Pelu Namastra Probosunu Nina Yuliana Ningsih, Maya Nirmalasari Idha Wijaya Nisya, Hima Choirun Noer Kasanah, Noer Nur Fadhilah Nur Rokhmat Nursyirwani Nursyirwani Pratiwinindya, Ratih Ayu Prayogo, Sugeng Purwanto Purwanto Putri Puspitasari R Sudradjat, R Rachmansyah Rachmansyah Raden Bagus Sugio Sumanta Rahmawati, Dwi Tyas Ratna Puspita, Ratna Retno Widaningroem REZA Adi ADI PRADANA Ria Azizah Tri Nuraini Rini Pramesti Risca Damayanti, Risca Risnawati, Ririn Riyadi Riyadi Rohendi Rohidi, Tjetjep Rohendi Rohidi, Tjetjep Rukayah Rukayah Rumi, Jalaluddin S. Soenarjo Sabillah, Masayu Selly Safia, Rina Anggraeni Sahli, Zamahsjari Salu, Vega Ricky SANTI NURBAITI Sebastian Margino Senny Helmiati Sesung, Rusdiyanto Setiawan, Feri Setyaningrum, Heny Setyaningrum, Ikha Sulis Setyobudi Setyobudi Shanie, Arsan Shatrie, Dikry N Shatrie, Dikry Novel Siti Amirah Budiastuti Sri Hartati Sri Iswidayanti Sri Iswidayati Sri Lestari, Yeni Sri Rejeki Sriyono Sriyono Subagiyo Subagiyo Suharno Suharno Suherman Suherman Sumarwati Sumarwati Sumaryanto Florentinus, Totok Sunarhadijoso Soenarjo Sunarto Sunarto Suparti Suparti Suryanti Retna Sari, Dyah Sutarman Sutarman Sutrisno sutrisno Suyono Suyono Syafii Syafii syakir syakir Syarif, Muh Ibnan Tanjung, Dailami Tjetjep Rohendi Rohidi, Tjetjep Rohendi Totok Sumaryanto Florentinus, Totok Sumaryanto Totok Sumaryanto, Totok Triani Widyaningrum Udi Utomo Umi Nur Sholikhah Utomo, Kasmidjo Budi W. Asmara W.Y. Rahman Wadiyo Wadiyo, Wadiyo Wardani, Anestia Widya Widaningtyas H, Adoniati Meyria Wijaya, Dhimayu Ichtiara Wijaya, Mas Benny Wilis Ari Ari Setyati1,2, Wilis Ari Wilis Ari Setyati Windi Amelia, Windi Wira Rahman Wira Y. Rahman Wisnu Nurcahyo Wulandari, Tita Yana, Rahma Husna Yatman, Teguh Mulyanto Yosita, Riesa Yudha Trinoegraha Adiputra Yulaida, Ita Yulius Docang Casessar Yuniarti, Ivana Yustiningrum, Giantari Ega